三丁胺

电解氟化制备全氟三丁胺研究

Study on Preparation of Perfluoro Tributylamine by Electrolytical Fluorination

结果表明：以溴苯与丙烯酸的反应为例，催化剂在130℃反应12h，三丁胺作为碱，催化剂用量为0.44mol%的钯含量，四丁基溴化铵作为溶剂的条件下具有较好的催化性能；

The results showed that the best condition contains 130 ℃, tributyl amine as alkali , tetrabutylammonium bromide as solvent , amount of catalyst 0.44 mol % Pd , 12 h.

结果表明：吡啶和N-三丁胺电解氟化的最佳值w分别为7%～10%和5%～7%，i分别为0.08～0.2A/cm2和0.03～0.05A/cm2；

Results show that the best values w of pyridine and N-tributylamine electrolysis fluorination are 7 ~ 10 % and 5 ~ 7 % respectively , I is 0.08 ~ 0.2 A / cm2 and 0.03 ~ 0.05 A / cm2 respectively ;

全氟三丁胺乳剂用于猴子换血的骨髓变化

Bone Marrow Changes of Monkey After Substitution With Perfluorotributylamine Emulsion

目的：评估国产全氟三丁胺（高碳液态氟化物）在复杂性视网膜脱离术中的应用价值。

Objective : To evaluate the clinical application value of perfluorotributylamine liquid ( PFTL ) made in China in the complicated retinal detachment .

全氟三丁胺在复杂性视网膜脱离术中的应用视网膜脱离术毕眼压测定的临床观察

The clinical application of perfluorotributylamine liquid in the complicated retinal detachment The observation of intraocular pressure measurement in the end of the retinal detachment surgery

实验结果表明，以三丁胺为萃取剂，正丁醇为稀释剂，相比在3~3.6的条件下，氯化钾的一次转化率较高。

The results indicate that , when we use Tri-n-butylamine as extraction reagent , n-butanol as diluent , and choose a phase ratio of 3 ~ 3.6 , we can get a higher first-stage conversion of potassium chloride .

绿脓杆菌对头孢三代及哌拉西林的耐药率10%～44%，肺炎克雷白杆菌对头孢三代及丁胺卡那霉素的耐药率11%～37%。

The antibiotic resistant rates were 10 % ~ 44 % for pseudomonas aeruginosa to cephalosporins ⅲ and piperacillin , and 11 % ~ 37 % for Klebsiella pneumoniae to cephalosporins ⅲ and amikacin .