苯甲酰氯
- 网络benzoyl chloride
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以荧光素和苯甲酰氯为原料制备了荧光素二苯甲酰酯,并用X射线单晶衍射法测定了晶体和分子结构。
The title compound has been prepared from the reaction of fluorescein and benzoyl chloride . Its crystal and molecular structure is determined by single crystal X-ray diffraction .
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苯甲酰氯亲核取代反应的热动力学研究
Study on the thermokinetics for nucleophilic substitution reactions of benzoyl chloride
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苯甲酰氯和D酒石酸反应生成D2,3二苯甲酰酒石酸酐,后者于丙酮水溶液中水解得到拆分剂D2,3二苯甲酰酒石酸。
The resolving reagent , D-2,3-dibenzoyl tartaric acid was obtained by hydrolyzation of D-2,3-dibenzoyl tartaric anhydride prepared by reaction of benzoyl chloride with D-tartaric acid .
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四丁基溴化铵(TBAB)为相转移催化剂、环己烷为溶剂,用己内酰胺和苯甲酰氯合成了N-苯甲酰基己内酰胺。
Using TBAB as phase transfer catalyst , N benzoyl caprolactam was synthesized from benzoyl chloride and caprolactam in cyclohexane .
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用棉纤维和三乙烯四胺为原料,以对二苯甲酰氯为交联剂,合成了新型多胺螯合纤维(CC-TC-TETA),并用红外(FT-IR)对其表征。
New polyamine chelation fibre ( cc-Tc-TETA ), which was attributed with FT-IR , was synthesized by cotton fibre and triethylene tetramine , with dibenzoyl as crosslinking agent .
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结果表明,将反应温度控制在35℃,催化剂K-1000用量为0.06%时,用苯甲酰氯作为阻聚剂可得到性能基本稳定的TDI三聚体产品。
The results showed that TDI trimer was attained when the reaction temperature was 35 ℃, the dosage of K-1000 was 0.06 % , and benzoyl chloride was used as inhibitor .
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用微晶纤维素和苯甲酰氯的超声反应合成了纤维素三苯甲酯(CTB),并将其涂敷于硅胶上,用作液相色谱手性固定相。
Cellulose tribenzoate chiral stationary phase ( CTB CSP ) was prepared by a modified procedure , in which CTB was synthesized by the ultrasonic reaction of benzoyl chloride with microcrystalline cellulose and then was coated on the silica gel .
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以1-苯基-3-甲基-5-吡唑啉酮为原料,二氧六环为溶剂,苯甲酰氯为酰化剂,合成得到了1-苯基-3-甲基-4-苯甲酰基-5-吡唑啉酮。
With solvent dioxane , acylating agent benzoyl chloride , 1-Phenyl-3-methyl-4-benzoyl-5-pyrazolone was prepared from 1-phenyl-3-methyl-5-pyrazolone .
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方法以氯苯和苯甲酰氯为原料,进行傅克酰化反应,合成出第一个反应中间体;
METHODS The intermediate 1 was synthesized via the friedel-crafts reaction between chlorobenzene and benzoyl chloride .
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它主要由苯甲酰氯和苯酚制备苯甲酸苯酯,然后重排、醚化所得。
It is based on phenol benzoate which is made from benzoyl chloride and phenol through rearrangement and etherification .
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在氯磺化反应中引入了四氯化碳溶剂,在反应后期加入氯化钠。利用苯甲酰氯与丙烯酸反应制备丙烯酰氯。
In the reaction of chlorosulfonation carbon tetrachloride was used as solvent , adding the sodium chloride in later stage reaction .
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以苯甲酰氯为原料,经酰化,还原,环合等反应合成左旋西替利嗪盐酸盐,反应总收率为8.05%。
Levocetirizine Dihydrochloride was prepared from benzoyl chloride by acidylation , hydrogenation , cyclization with an overall yield of 8.05 % .
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研究了三氯甲苯和氯乙酸在催化剂存在下反应生成氯乙酰氯和苯甲酰氯的工艺条件。
The reaction of benzotrichloride and chloroacetic acid to form chloroacetyl chloride and benzoyl chloride in the presence of catalyst was studied .
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苯环上氯取代会降低化合物的生物可降解性苯甲酰氯亲核取代反应的热动力学研究
The chloro group on benzene was shown to lower the biodegradability . STUDY ON THE THERMOKINETICS FOR NUCLEOPHILIC SUBSTITUTION REACTIONS OF BENZOYL CHLORIDE
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叙述了苯甲酰氯的性质、合成工艺路线、实验室和工业制法,产品规格及其分析方法。并对其深加工产品及其应用进行了概述。
In this paper the synthetic methods and properties of benzoyl chloride are introduced , and its downstream products and its application are stated .
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1羟基咪唑类(Ⅰ)在三乙胺存在下与苯甲酰氯反应制得新型的活性单酯1苯甲酰氧咪唑类(Ⅱ)。
1 Benzoyloxyimidazoles (ⅱ) as new active esters , were prepared by the reaction of 1 hydroxyimidazoles (ⅰ) with benzoyl chloride in the presence of triethylamine .
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在催化剂存在下,以固体氰化钠和苯甲酰氯为原料合成苯甲酰氰,研究了反应条件对收率的影响。优化条件下收率达72%(以苯甲酰氯计)。
Benzoyl cyanide was synthesized by the reaction of sodium cyanide with benzoyl chloride in a polar compounds as a catalyst with the yield of 72 % .
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研究表明:苯甲酰氯衍生反应条件温和,样品处理简单,分离时间短,灵敏度高。
It was found that : The condition of the derivatization is moderation , sample pretreatment is relatively simple , the retention time is short and the analytical method is more sensitive .
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以丙烯酸为偶联剂制备二氧化硅/聚丙烯酸-丙烯酰胺复合材料利用苯甲酰氯与丙烯酸反应制备丙烯酰氯。
Synthesis of SiO_2 / P ( AA-AM ) Core / Shell Hybrid Material Using Acrylic Acid as Coupling Agent The compound of acryloyl chloride was synthesized by benzoyl chlorid and crylic acid .
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将壳聚糖在甲磺酸中充分溶胀后,与3,4,5-三甲氧基苯甲酰氯反应,得到壳聚糖改性高分子紫外线吸收剂。
Chitosan is dissolved in the methylsulfonic acid and reacted with 3,4,5-trimethoxy benzoyl chloride with certain molar ratio to bond 3,4,5-trimethoxy benzoic acid , which bears excellent UV absorption performance , onto the chain of chitosan .
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研究了在苯甲酸乙酯、盐酸羟胺和氯化铁反应体系中间接测定苯甲酰氯的酯化分光光度法,探讨了反应机理和络合物的结构组成。
An indirect esterified spectrophotometric method for the determination of benzoyl chloride is studied in the reactive system of ethyl benzoate , oxammonium hgdrochloride and iron chloride . The mechanism of reaction and the composition of complex are discussed .
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采用低温溶液法共缩聚反应合成了对苯二甲酰氯(TPC)摩尔分数为0.05~0.15的改性间位芳香族聚酰胺(PMIA)共聚物。
Modified meta-aramid ( PMIA ) copolymer with TPC mole fraction of 0.05 ~ 0.15 was prepared by low-temperature-solution polycondensation in DMAc .
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以双酚A(BPA)和间苯二甲酰氯(IC)作为反应体系,采用界面缩聚的方法得到了NF-1(nanofiltrationmembrane)复合纳滤膜。双酚A多段滴流床反应气提模型试验分析
Composite nanofiltration membrane ( NF1 ) was obtained by the interfacial polymerization using bisphenolA ( BPA ) and isophthaloyl chloride ( IC ) . ANALYSIS OF REACTION AND STRIPPING PROCESS WITH MULTI STAGES TRICKLE BED REACTOR IN THE MODEL TEST OF BPA
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用气相色谱法测定对苯二甲酰氯中的杂质
Determination of Impurities in Terephthalic Acid Chloride by Gas Chromatography
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三相相转移催化合成对苯二甲酰氯的研究
Study on synthesis of terephthaloyl dichloride by triphase phase-transfer catalysis
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对苯二甲酰氯合成钼酸银修饰电极的制备及其电化学性能研究
Studies on the Preparation and Electrochemical Properties of Argentic Molybdate Compound Film Modified Electrode
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对苯二甲酰氯是重要的有机合成中间体,在合成化学领域起着非常重要的作用。
Terephthaloyl dichloride is a useful organic synthetic intermediate , and plays an important role in organic chemistry field .
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本文通过低温溶液法,采用间苯二甲酰氯、2,6-萘二甲酰氯作第三单体,进行共聚改性。
In this paper , we respectively used isophthalate dichloride and 2,6-naphthalene dichlorides as third monomers to modify the polyester , and prepared two kind of copolyesters , which have kink chain in the main chain of polymers .
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以二苯醚与苯甲酰氯为原料,合成了一种新型的激光光敏刺&4-苯氧基二苯甲酮(PBZP)。
A new photoinitiator , 4-phenoxy benzophenone ( PBZP ), was synthesized and characterized using diphenyl ether and benzoyl chloride as raw material .
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2-(4-三氟甲基苯氧基)对苯二甲酰氯的合成与表征
Synthesis and Characterization of 2 - ( 4-Trifluoromethylphenoxy ) terephthalyl Chloride