Acyl Chloride

The slower acyl chloride dropped , the higher the yield will be .

酰氯的滴加速度愈慢，产品的收率就愈高。

Maltitol fatty acid ester was prepared with maltitol and fatty acyl chloride .

以麦芽糖醇和脂肪酰氯为主要原料合成麦芽糖醇脂肪酸酯。

Water is avoided to take with acyl chloride .

酰氯化物切忌带水。

Solid state polymerization of poly ( ethylene terephthalate ) through acyl chloride method

聚对苯二甲酸乙二酯的酰氯法固态聚合

Synthetic Study of Glycyl-Glycyl-Valine Tripeptide Using The Way of Acyl Chloride

酰氯法合成甘氨酰-甘氨酰-缬氨酸三肽的实验研究

The method of acyl chloride was better than the method of active ester for its high efficiency and convenient operation .

酰氯法反应速率快、操作简便，优于活化酯法。

Study on the Reduction of Acyl Chloride by Tributyltin Hydride on Pd / C Catalyst

三丁基锡氢化物在Pd/C催化下还原酰氯的反应研究

Preparation of Borohydride Anion Exchange Resin ( BER ) and Reductions of Carbonyl Group and Acyl Chloride Compounds

硼氢阴离子交换树脂的制备及其对羰基、酰氯化合物的还原

The reaction of twenty kinds of Fmoc-AA-OH linked to Wang resin using methods of acyl chloride or active ester was studied in solid-phase peptide synthesis .

在多肽固相合成中，分别采用酰氯法和活化酯法，研究了20种Fmoc-氨基酸与Wang树脂的连接反应。

Pinonic acyl chloride was reacted with diethyl amine to synthesize N , N-diethyl-pinonic amide .

蒎酮酸经过酰氯化后再和二乙胺反应，合成了可能有生物活性的N，N-二乙基蒎酮酸酰胺。

Pyridine can improve the ability of acylation when it complex with acyl chloride . The theory yield is high but aftertreatment is difficult and real yield is very low .

吡啶既可做溶剂又可中和氯化氢，还可与酰氯形成络和物而增强酰化能力，理论产率很高，但后处理困难，实际产率反而很低。

Liposoluble tea polyphenols ( LTP ) with varying aliphatic groups were synthesized by reaction of aliphatic acyl chloride and tea polyphenol ( TP ) .

通过脂肪酰氯与茶多酚（TP）的反应，制备出了一系列含不同直链脂肪基团的脂溶性茶多酚（LTP）。

Peptides are traditionally synthesized in liquid phase , such methods are DCC , mixed anhydrides , acyl chloride and azide etc. , which provide more choices for peptides synthesis .

传统的肽类合成多采用液相化学合成，常用的包括碳二亚胺（DCC）法，混合酸酐法、酰氯法、叠氮物法等等，为多肽的合成提供了多种选择。

To seek a nicotinic derivative with effect , safety and less adverse effect , nicotinyl salicylic acid was synthesized from nicotinic acid with salicylic acid by employing the acyl chloride method .

为寻找降血脂作用强、不良反应轻、安全有效的烟酸衍生物，以烟酸和水杨酸为原料，采用酰氯法经过二步合成了烟酸的衍生物烟酰水杨酸。

For arginine , the yield was improved to nearly 80 % by using weakly polar solvent such as DCM and simultaneously increasing the reaction time to 20 h in the method of acyl chloride .

在酰氯法中，对于精氨酸，选择弱极法溶剂如DCM，延长反应时间至20h，连接效率接近80%。

40 products are synthesized by the variation of modification parameters , which are the species of lignin , reaction ratios of Mannich Reaction and acylation , and the number of carbon atoms in aliphatic acyl chloride .

通过改变木质素的种类、酰化反应的投料比以及脂肪酰氯的碳链长度等参数，合成了40只不同的改性木质素磺酸盐产品。

Methyl-furoate is synthesized from furfural by Cannizzaro reaction , acyl chloride reaction and esterification . It showed that the time of esterification is only 2.5 hours and the yield can reach 85.0 % .

以糠醛为起始原料，通过康尼查罗反应、酰氯化和酯化反应合成了糠酸甲酯，实验结果表明：酯化反应时间2.5h，糠酸甲酯收率可达85.0%。

The experimental results indicate that the average substitution degree of acylation of chitosan depends on volume ratio of pyridine to chloroform in the reaction medium , chain length of the acyl chloride , and molecular weight of the chitosan .

实验结果表明：壳聚糖的酰化取代度主要取决于反应介质吡啶／氯仿用量比、酰化试剂的链长和壳聚糖分子量。

N-acylation takes place from ester as acylating agent and amine , which avoids the reaction of esterolysis and chlorination . Compared to the former method using irritant acyl chloride as acylating agent , this new process shortens the reaction steps and avoids pollution .

N-酰化反应，直接用酯作为酰化试剂与胺反应，代替了有强烈刺激性的酰氯，避免了酯的水解、氯化反应，既减少了反应步骤，又有利于清洁生产；

Structural Determination of the By & Product in Preparing Acyl Urea by Reaction of Acyl Chloride with Lead Cyanate

由酰氯与氰酸铅制备酰基脲反应中副产物的结构测定

The optimal parameters of acyl chlorination were selected as follows : oxalyl chloride as acyl chloride reagent , DMF as catalyst , the yield was 90.7 % .

酰氯化反应条件为：草酰氯为酰氯化试剂，DMF为催化剂，收率90.7%。

Synthesis of acyl azide from aldehyde , or acylhydrazine , or carboxylic acid , or acyl chloride , or anhydride , or ester is introduced in this paper .

介绍了由醛、酰肼、羧酸、酰氯、酐或酯合成酰基叠氮化合物方法。