肉桂酰氯
- 网络cinnamoyl chloride;Cinnamyl chloride
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制备了以超细二氧化硅为载体的氰乙基化可溶性蛋白质-钯催化剂,研究了它在三丁基芳基锡和取代肉桂酰氯的偶联反应中的催化行为。
The activity of the catalyst used for the synthesis of Chalcoues in the cross-coupling reaction of tributylaromatic tin and substituted cinnamoyl chlorides was investigated .
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第一步将肉桂酸制成肉桂酰氯,第二步将肉桂酰氯与苄醇反应制得肉桂酸苄酯。结构经IR,1HNMR和MS确证。
Benzyl cinnamate was synthesized by a two-step reaction : cinnamic acid reacted with thionyl chloride giving cinnamyl chloride and cinnamyl chloride was then reacted with benzyl alcohol giving benzyl cinnamate whose structure was characterized by IR , 1H NMR and MS.